HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyridine → HCID 15453908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | HCID 15453907 | HCID 15453907 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15453908 | HCID 15453908 | 48.1% |
Reaction Steps
5-Bromoacetyl-2-(phthalimidomethyl)thiophene (0.80 g) and 2-aminopyridine (0.23 g) were dissolved in anhydrous ethanol (50 ml) and heated under reflux for 6 hours. The resulting crystals were collected by filtration and purified by a silica gel column chromatography (chloroform:methanol=100:1) to give 0.38 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090804 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-5d6e879fbf9248ecba785528d4f2c017 |
| Source note | uspto-grants-2000_07 |