Thiobenzamide → HCID 9820802, compound

HRID 2288783Notes

Reaction equation

HRID 2288783 reaction equation
[Br:1][CH:2]1[CH2:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:11]#[CH:12])[CH:8]=2)[C:3]1=[O:13].[C:14]([NH2:22])(=[S:21])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[BrH:1].[C:11]([C:7]1[CH:6]=[CH:5][C:4]2[C:3]3([OH:13])[N:22]=[C:14]([C:15]4[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=4)[S:21][CH:2]3[CH2:10][C:9]=2[CH:8]=1)#[CH:12]

Participants

3

Reactant 2

HCID 683563ThiobenzamideHCID 21702060HCID 21702060, compound

Product 1

HCID 9820802HCID 9820802, compound

Procedure

This compound is prepared analogously to the process described in Example 1c using 2-bromo-5-ethynylindan-1-one and thiobenzamide; melting point: 133-134° C. (dec.).

Workup

  1. customThis compound is prepared analogously to the process

Sources & evidence

ORD record
ord-b9384b4611624042a2304fe4d0a15d46
Source dataset
uspto-grants-2000_07
Patent number
US06090833

Reaction notes

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