HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetylbenzoic Acid → 4-Acetylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetylbenzoic Acid | HCID 11470 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 4-Acetylbenzoyl chloride | HCID 13409603 | — |
Reaction Steps
120 mmol of thionyl chloride are added to 600 mmol of 4-acetylbenzoic acid in 150 ml of toluene. The reaction mixture is heated at reflux for 3 hours and then cooled. The solvent is evaporated off. The product is used without any other treatment.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090837 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-719fe9b2a7304aab88ae7cba14527f68 |
| Source note | uspto-grants-2000_07 |