HRID2288886

反应详情

EQUATION

反应方程式

HRID 2288886 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 4-(4-fluorophenoxy)-2-allylphenol (2.30 g, 9.42 mmol) and 5% Pd/C (0.90 g) in ethyl acetate (30 mL) was stirred under H2 atmosphere for 3 h at room temperature. The reaction mixture was filtered through a short pad of silica gel and concentrated in vacuo to afford the title compound which was used as is.

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered through a short pad of silica gel
  2. concentrationconcentrated in vacuo