HRID2288892

反应详情

EQUATION

反应方程式

HRID 2288892 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

4-Allyl-5-hydroxy-N-neopentylindole (Step C; 1.0 g, 3.54 mmol) was taken up in 25 mL ethyl acetate and hydrogenated (1 atm) at ambient temperature using 5% palladium on charcoal (40 mg) for 2 hours. The reaction was filtered through celite and concentrated in vacuo to provide the title compound which was used without further purification.

WORKUP

后处理

  1. customat ambient temperature
  2. customfor 2 hours
  3. filtrationThe reaction was filtered through celite and
  4. concentrationconcentrated in vacuo