HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 15888339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 15888338 | HCID 15888338 | — |
| Product | HCID 15888339 | HCID 15888339 | 48% |
Reaction Steps
[6-Methoxy-2-(4-methoxyphenyl)benzo[b]thiophen-3-yl][4-(cyclohexanoyloxyethoxy)phenyl]methanone (1.25 g, 2.3 mmol) was converted to the title compound by the procedure of Example 3 using 400 mg (7.0 mmol) of ethanethiol and 920 mg (7.00 mmol) of aluminum chloride (0.92 g, 7.00 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090843 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-2ecab449afb2466a8716316c03f39616 |
| Source note | uspto-grants-2000_07 |