HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 15888351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 15888350 | HCID 15888350 | — |
| Product | HCID 15888351 | HCID 15888351 | 66% |
Reaction Steps
[6-Methoxy-2-(4-methoxyphenyl)benzo[b]thiophen-3-yl][4-(2-hydroxy-3-[3-methylpiperidinyl]propoxy)phenyl]methanone (540 mg, 1.0 mmol) was converted to 340 mg of the title compound by the procedure of Example 32 using 360 mg (4.9 mmol) of ethanethiol and aluminum chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090843 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-aaee0186f7cf415db53cee21b8055286 |
| Source note | uspto-grants-2000_07 |