Hydroxylamine → HCID 53795025, compound

HRID 2288929Notes

Reaction equation

[C:1]1([CH2:13][CH2:14][NH:15][S:16]([CH2:19][C:20]([O:22]C)=O)(=[O:18])=[O:17])[CH:6]=[CH:5][C:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[CH:3][CH:2]=1.[NH2:24][OH:25]>>[OH:25][NH:24][C:20](=[O:22])[CH2:19][S:16]([NH:15][CH2:14][CH2:13][C:1]1[CH:6]=[CH:5][C:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[CH:3][CH:2]=1)(=[O:18])=[O:17]

Participants

Reactant 2

HCID 787Hydroxylamine

HCID 131721882HCID 131721882, compound

Product 1

HCID 53795025HCID 53795025, compound

Procedure

In a manner similar to Example 1 (b), methyl 2-({[2-(biphen4-yl)ethyl]amino}sulfonyl)acetate was reacted with hydroxylamine to give the title compound as a colourless solid.

Sources & evidence

ORD record: ord-2c2dd11a6c1747f8a56b1330ec51e255
Source dataset: uspto-grants-2000_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06090852

Reaction notes

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