Hydroxylamine → HCID 44445388, compound

HRID 2288931Notes

Reaction equation

HRID 2288931 reaction equation
[CH3:1][N:2]([CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][C:16]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[CH:15][CH:14]=1)[S:3]([CH2:6][C:7](OC)=[O:8])(=[O:5])=[O:4].[NH2:25][OH:26]>>[OH:26][NH:25][C:7](=[O:8])[CH2:6][S:3]([N:2]([CH3:1])[CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][C:16]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[CH:15][CH:14]=1)(=[O:5])=[O:4]

Participants

3

Reactant 2

HCID 787HydroxylamineHCID 131721883HCID 131721883, compound

Product 1

HCID 44445388HCID 44445388, compound

Procedure

In a manner similar to Example 1 (b), methyl 2-({methyl-[2-(biphen-4-yl)ethyl]amino}sulfonyl)acetate was reacted with hydroxylamine to give the title compound as a colourless solid.

Sources & evidence

ORD record
ord-3426d409d3994687b2e6161681351caa
Source dataset
uspto-grants-2000_07
Patent number
US06090852

Reaction notes

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