Hydroxylamine → HCID 54352566, compound

HRID 2288935Notes

Reaction equation

C[O:2][C:3](=O)[CH2:4][S:5]([N:8]([CH3:23])[CH2:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[CH:21]=[CH:20][C:19]([Cl:22])=[CH:18][CH:17]=2)=[CH:12][CH:11]=1)(=[O:7])=[O:6].[NH2:25][OH:26]>>[OH:26][NH:25][C:3](=[O:2])[CH2:4][S:5]([N:8]([CH3:23])[CH2:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[CH:21]=[CH:20][C:19]([Cl:22])=[CH:18][CH:17]=2)=[CH:12][CH:11]=1)(=[O:7])=[O:6]

Participants

Reactant 2

HCID 787Hydroxylamine

HCID 18702049HCID 18702049, compound

Product 1

HCID 54352566HCID 54352566, compound

Procedure

In a manner similar to Example 1 (b), methyl-2-({methyl[(4'-chlorobiphenyl-4-yl)methyl]amino}sulfonyl)acetate was reacted with hydroxylamine to give the title compound as a colourless solid.

Sources & evidence

ORD record: ord-03cfa034e79e404bb52233a38d31eeab
Source dataset: uspto-grants-2000_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06090852

Reaction notes

Loading…