Hydroxylamine → HCID 131721885, compound

HRID 2288937Notes

Reaction equation

HRID 2288937 reaction equation
[CH3:1][N:2]([CH2:11]/[CH:12]=[CH:13]/[C:14]1[CH:19]=[CH:18][C:17]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:16][CH:15]=1)[S:3]([CH2:6][C:7](OC)=[O:8])(=[O:5])=[O:4].[NH2:26][OH:27]>>[OH:27][NH:26][C:7](=[O:8])[CH2:6][S:3]([N:2]([CH3:1])[CH2:11]/[CH:12]=[CH:13]/[C:14]1[CH:19]=[CH:18][C:17]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:16][CH:15]=1)(=[O:5])=[O:4]

Participants

3

Reactant 2

HCID 787HydroxylamineHCID 18702053HCID 18702053, compound

Product 1

HCID 131721885HCID 131721885, compound

Procedure

In a manner similar to Example 1 (b), methyl 2-({methyl[3-(1,1'-biphenyl-4-yl)-trans-prop-2-enyl]amino}sulfonyl)acetate was reacted with hydroxylamine to give the title compound as a colourless solid.

Sources & evidence

ORD record
ord-1d39b3b2177b4a0a8cebaf826f6f5b18
Source dataset
uspto-grants-2000_07
Patent number
US06090852

Reaction notes

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