Hydroxylamine → HCID 131721886, compound

HRID 2288938Notes

Reaction equation

[CH3:1][N:2]([CH2:11]/[CH:12]=[CH:13]/[C:14]1[CH:19]=[C:18]([CH3:20])[C:17]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)=[CH:16][CH:15]=1)[S:3]([CH2:6][C:7](OC)=[O:8])(=[O:5])=[O:4].[NH2:27][OH:28]>>[OH:28][NH:27][C:7](=[O:8])[CH2:6][S:3]([N:2]([CH3:1])[CH2:11]/[CH:12]=[CH:13]/[C:14]1[CH:19]=[C:18]([CH3:20])[C:17]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)=[CH:16][CH:15]=1)(=[O:5])=[O:4]

Participants

Reactant 2

HCID 787Hydroxylamine

HCID 131721887HCID 131721887, compound

Product 1

HCID 131721886HCID 131721886, compound

Procedure

In a manner similar to Example 1 (b), methyl 2-({methyl-[3-(2-methylbiphen-4-yl)-trans-prop-2-enyl]amino}sulfonyl)acetate was reacted with hydroxylamine to give the titled compound as a colourless solid.

Sources & evidence

ORD record: ord-86258b3ee95d42d888f8e553f25b421c
Source dataset: uspto-grants-2000_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06090852

Reaction notes

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