HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86755555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 57034816 | HCID 57034816 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86755555 | HCID 86755555 | — |
Reaction Steps
To a solution of the compound (1.48 g), which had been obtained in (1), in anhydrous dichloromethane (8 ml), trifluoroacetic acid (4 ml) was added dropwise under ice cooling. The reaction mixture was then treated in a similar manner to that described in Referential Example 16-(2), whereby the title compound was obtained. The product was provided for use in the subsequent reaction without isolation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090802 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-482e5d41b60947969276c8d78c424658 |
| Source note | uspto-grants-2000_07 |