HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichlorobenzene → HCID 14677683, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichlorobenzene | HCID 7239 | — |
| Reactant | HCID 12941055 | HCID 12941055 | — |
| Product | HCID 14677683 | HCID 14677683 | — |
Reaction Steps
A solution of methyl 4-alloxyphenylacetate (3.1 grams) in dry ortho-dichlorobenzene (50 mL) was refluxed for 25 hours. The solvent was removed under reduced pressure, and the residue was purified by chromatography (silica gel, 50% methylene chloride in hexane) to afford the tittle compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090836 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-fad1b842688347a0a7dd872f6dfd9aa1 |
| Source note | uspto-grants-2000_07 |