1,3-Benzenediol, propyl- → HCID 18701977, compound

HRID 2289119Notes

Reaction equation

HRID 2289119 reaction equation
[F:1][C:2]([F:9])([F:8])[CH2:3][CH2:4][C:5](O)=[O:6].[CH2:10]([C:13]1[C:19]([OH:20])=[CH:18][CH:17]=[CH:16][C:14]=1[OH:15])[CH2:11][CH3:12]>OS(C(F)(F)F)(=O)=O>[OH:15][C:14]1[CH:16]=[CH:17][C:18]([C:5](=[O:6])[CH2:4][CH2:3][C:2]([F:9])([F:8])[F:1])=[C:19]([OH:20])[C:13]=1[CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 2620601,3-Benzenediol, propyl-HCID 27770854,4,4-Trifluorobutanoic acid

Product 1

HCID 18701977HCID 18701977, compound

Reagents, catalysts & solvents 1

HCID 62406Trifluoromethanesulfonic acidSolvent

Procedure

Using the procedure in Example 51, step 1, 4,4,4-trifluoro-butyric acid and 2-(n-propyl)resorcinol were condensed in triflic acid to form 1,3-dihydroxy-2-(n-propyl)-4-(4,4,4-trifluorobutyryl)benzene

Sources & evidence

ORD record
ord-6464cb6480de4efc979d3d029cae9c82
Source dataset
uspto-grants-2000_07
Patent number
US06090836

Reaction notes

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