beta-Phenylisovaleric acid → HCID 18701946, compound

HRID 2289134Notes

Reaction equation

HRID 2289134 reaction equation
[CH3:1][C:2]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)([CH3:7])[CH2:3][C:4]([OH:6])=O.[CH2:14]([C:17]1[C:23]([OH:24])=[CH:22][CH:21]=[CH:20][C:18]=1[OH:19])[CH2:15][CH3:16]>OS(C(F)(F)F)(=O)=O>[OH:19][C:18]1[CH:20]=[CH:21][C:22]([C:4](=[O:6])[CH2:3][C:2]([CH3:1])([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH3:7])=[C:23]([OH:24])[C:17]=1[CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 13890beta-Phenylisovaleric acidHCID 2620601,3-Benzenediol, propyl-

Product 1

HCID 18701946HCID 18701946, compound

Reagents, catalysts & solvents 1

HCID 62406Trifluoromethanesulfonic acidSolvent

Procedure

Using the procedure in Example 51, step 1; 3-methyl-3-phenylbutyric acid and 2-(n-propyl)resorcinol were condensed in triflic acid to form 1,3-dihydroxy-4-(3-methyl-3-phenylbutyryl)-2-(n-propyl)benzene.

Sources & evidence

ORD record
ord-1bffa887af344da49072dd6916f163bd
Source dataset
uspto-grants-2000_07
Patent number
US06090836

Reaction notes

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