Aluminium lithium hydride → HCID 70269844, compound

Participants

Reaction Steps

A mixture of 0.6 g of lithium aluminum hydride and 60 ml of diethyl ether was kept at -5° to -10° C., and a solution of the ester derivative (2.12 g) obtained in Step 8 in 50 ml of diethyl ether was added thereto dropwise, followed by stirring at that temperature for 2 hours. The reaction mixture was poured into ice-water and extracted with diethyl ether. The extract was washed with water and distilled to remove the solvent to obtain 1.51 g (70.01%) of the titled compound.

Provenance & Evidence