HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18697997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 18698059 | HCID 18698059 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18697997 | HCID 18697997 | — |
Reaction Steps
Ethyl acetate saturated with gaseous HCl was added to a solution of 1-(4-chlorophenylsulphonyl)-4-[1-(t-butoxyoxycarbonyl)piperazine-4-ylcarbonyl]piperidine (1.10 g) in ethyl acetate (25 ml). The reaction was stirred at room temperature for 2 hours. Solvent was removed by evaporation to give the crude 1-(4-chlorophenylsulphonyl)-4-(4-piperazinylcarbonyl)piperidine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06093718 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-0e12433721ea452abd7894ba12a986de |
| Source note | uspto-grants-2000_07 |