HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 23078411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | HCID 23078262 | HCID 23078262 | — |
| Product | HCID 23078411 | HCID 23078411 | 59% |
Reaction Steps
A hydrochloric acid/methanol solution (30 ml) was added to 6-methoxy-4-(2-methyl-quinolin-3-yloxy)-7-(2-morpholin-4-yl-ethoxy)-quinoline (compound 365) (748 mg), and the mixture was stirred at room temperature for one hr. The solvent was removed by distillation under the reduced pressure to give the title compound (900 mg, yield 59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560558B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-a61a77b601f241fe85d7f156fbfaa5c4 |
| Source note | uspto-grants-2009_07 |