HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 1-(3-(hydroxymethyl)phenyl)-5-oxopyrrolidine-3-carboxylate → HCID 131724724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 1-(3-(hydroxymethyl)phenyl)-5-oxopyrrolidine-3-carboxylate | HCID 22591870 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131724724 | HCID 131724724 | — |
Reaction Steps
To a solution of methyl 1-(3-(hydroxymethyl)phenyl)-5-oxopyrrolidine-3-carboxylate in CH2Cl2 was added pyridinium chlorochromate (PCC). The reaction was stirred at room temperature overnight. The mixture was then filtered through a pad of celite. The filtrate was concentrated in vacuo and the desired product was obtained after silica gel chromatograph. MS (ES+): 248.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849639B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-c1b050261f1c457e9455ca6df6938a6d |
| Source note | uspto-grants-2005_02 |