HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 18698144, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 54729592 | HCID 54729592 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 18698144 | HCID 18698144 | — |
Reaction Steps
2.0 g of compound B from Example 1e) were reacted with phosphorus oxychloride analogously to 1f). After chromatography using heptane/ethyl acetate (4:1) on silica gel, 1.5 g of product were isolated; m.p. 116-118° C. (from petroleum ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06093730 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-910cec84c56e4d939581817011ba2744 |
| Source note | uspto-grants-2000_07 |