m-Chloroperbenzoic acid → HCID 178522921, compound

HRID 2290020Notes

Reaction equation

HRID 2290020 reaction equation
[Cl:1][C:2]1[CH:27]=[CH:26][C:5]([CH2:6][NH:7][C:8]([C:10]2[CH:11]=[N:12][C:13]3[C:18]([C:19]=2[OH:20])=[CH:17][C:16]([S:21][CH2:22][CH2:23][OH:24])=[CH:15][C:14]=3[F:25])=[O:9])=[CH:4][CH:3]=1.ClC1C=CC=C(C(OO)=[O:36])C=1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][NH:7][C:8]([C:10]2[CH:11]=[N:12][C:13]3[C:18]([C:19]=2[OH:20])=[CH:17][C:16]([S:21]([CH2:22][CH2:23][OH:24])=[O:36])=[CH:15][C:14]=3[F:25])=[O:9])=[CH:26][CH:27]=1

Participants

3

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 178522920HCID 178522920, compound

Product 1

HCID 178522921HCID 178522921, compound

Procedure

This compound was prepared from N-(4-chlorobenzyl)-8-fluoro-4-hydroxy-6-[(2-hydroxyethyl)sulfanyl]-3-quinolinecarboxamide (Example No. 171) and an equimolar amount of m-chloroperbenzoic acid according to a procedure similar to described in Example 175.

Sources & evidence

ORD record
ord-98d6e10dab714ee393ee86a69b813690
Source dataset
uspto-grants-2000_07
Patent number
US06093732

Reaction notes

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