HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 20231959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 14853009 | HCID 14853009 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20231959 | HCID 20231959 | — |
Reaction Steps
A stirred mixture of 5-cyano-2-methylindan-1-one (9.36 g), glacial acetic acid (90 ml) and concentrated hydrochloric acid (90 ml) was heated under reflux for 20 hours to afford 5-carboxy-2-methylindan-1-one, m.p. 189°-194° C. (from aqueous ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04616013 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-9a2cf8d5aeaf456ea8153ec2013d8978 |
| Source note | uspto-grants-1986_10 |