HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 20232224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 3-Methoxy-10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-one | HCID 20232266 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20232224 | HCID 20232224 | — |
Reaction Steps
In a manner similar to that described in the preceding examples, 0.5 gram (13 millimoles) of sodium borohydride was added to a solution of 1 gram (43 millimoles) of 10,11-dihydro-3-methoxy-5H-dibenzo[a,d]cyclohepten-5-one in 20 milliliters of ethanol with an added drop of 40 percent sodium hydroxide solution and the mixture heated overnight to obtain 10,11-dihydro-3-methoxy-5H-dibenzo[a,d]cyclohepten-5-ol (5-hydroxy intermediate compound) in the reaction mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04616023 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-aeb4b3cf5d7c4defad93e85ee09fb93a |
| Source note | uspto-grants-1986_10 |