HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 20232011, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 20232094 | HCID 20232094 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20232011 | HCID 20232011 | 15% |
Reaction Steps
A solution of 6-(4-chlorophenyl)-5-methyl-3-methylthio-1,2,4-triazine (32.4 g) and hydrazine hydrate (40.8 g) in ethanol (110 ml) was heated for 2 hours. After cooling, the precipitates were collected by filtration, washed with ethanol, dried and recrystallized from ethanol to give 6-(4-chlorophenyl)-3-hydrazino-5-methyl-1,2,4-triazine (4.54 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04616014 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-e3980300259b431ab5fe7c237b2fef2a |
| Source note | uspto-grants-1986_10 |