Sulfate Ion → HCID 20232480, compound

HRID 2290463Notes

Reaction equation

HRID 2290463 reaction equation
NC1C=CC(CC(OCCCC)=O)=CC=1.[N:16]1([C:22]2[CH:27]=[CH:26][C:25]([CH2:28][C:29]([O:31][CH2:32][CH2:33]CC)=[O:30])=[CH:24][CH:23]=2)[CH2:21][CH2:20][NH:19][CH2:18][CH2:17]1.S([O-])([O-])(=O)=O>>[N:16]1([C:22]2[CH:23]=[CH:24][C:25]([CH2:28][C:29]([O:31][CH2:32][CH3:33])=[O:30])=[CH:26][CH:27]=2)[CH2:17][CH2:18][NH:19][CH2:20][CH2:21]1

Participants

4

Reactant 3

HCID 1117Sulfate IonHCID 12238924HCID 12238924, compoundHCID 20232546HCID 20232546, compound

Product 1

HCID 20232480HCID 20232480, compound

Procedure

In analogous manner, with the use of n-butyl 4-aminophenylacetate, there is prepared n-butyl 4-(piperazin-1-yl)-phenylacetate; yield 52% of theory of sulphate; m.p. 197°-199° C.

Sources & evidence

ORD record
ord-07bc741cf6564305be7b59a04460a68a
Source dataset
uspto-grants-1986_10
Patent number
US04616086

Reaction notes

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