HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine → HCID 43721984, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | 2-Chloro-6-methoxypyridine | HCID 87009 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 43721984 | HCID 43721984 | 40.2% |
Reaction Steps
In the same reacting apparatus as in Example 1, 20 g of 2-chloro-6-methoxypyridine, 25 g of n-propylamine and 80 ml of water were charged and they were subjected to reacting each other at 180° C. for 5 hours. After completion of the reaction, the similar experimental procedure was carried out to give 9.3 g of 2-methoxy-n-propylaminopyridine of b.p. 90°-91° C./4 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04617397 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-f87c938b6af440639f9e256aa717beac |
| Source note | uspto-grants-1986_10 |