HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 1,3-Benzodioxol-5-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Mitomycin A | HCID 19972 | — |
| Product | 1,3-Benzodioxol-5-amine | HCID 84310 | — |
Reaction Steps
This compound was prepared by the procedure described in Example 1, except that the potassium carbonate was omitted. From 80 mg. of mitomycin A and 0.1 ml. of 3,4-methylenedioxyaniline was obtained 50 mg. (48% yield) of the desired product having a melting point of 86°-88° C. (decomposition) and providing the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04617389 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-1cbc687263b44bd091db86cd79eaae41 |
| Source note | uspto-grants-1986_10 |