Bromotrimethylsilane → HCID 53836494, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 3.2 g of monoethyl N-[2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenyl]-N-methylaminoethylphosphonite and 10 g of trimethylbromosilane is stirred for 18 hours at 20° C. Excess trimethylbromosilane is removed by evaporation and the residue is then taken up in ethanol and the solution is evaporated, affording as residue a yellow oil which crystallises from ether. Yield: 2.14 g (71.3% of theory) of the title compound with a melting point of 161°-164° C.

Provenance & Evidence