Water → HCID 13386052, compound

Participants

Reaction Steps

A solution of 6-(4-acetamidophenyl)-5-methyl-4,5-dihydro-1,2,4-triazin-3(2H)-one (0.5 g) and N-chlorosuccinimide (0.41 g) in dimethylformamide (7 ml) was stirred at 40° C. for 3 hours and then poured into water. The thus-produced crsytals were collected by filtration, washed with water and dried to give 6-(4-acetamido-3-chlorophenyl)-5-methyl-4,5-dihydro-1,2,4-triazin-3(2H)-one (0.331 g).

Provenance & Evidence