HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanesulfonyl chloride → Ethanesulfonic acid;7-hydroxy-3,4-dimethylchromen-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanesulfonyl chloride | HCID 11667 | — |
| Reactant | 7-hydroxy-3,4-dimethyl-2H-chromen-2-one | HCID 5412990 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | Ethanesulfonic acid;7-hydroxy-3,4-dimethylchromen-2-one | HCID 86741079 | — |
Reaction Steps
5.0 g of 7-hydroxy-3,4-dimethylcoumarin were dissolved in 20 ml of H2O/1.1 g of NaOH at room temperature, while stirring, and 3.4 g of ethanesulfonyl chloride were added. The mixture was stirred overnight, and the precipitate was filtered off under suction and recrystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618622 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-6ef9b4ad9f104ef58760f70b6ee8b4cf |
| Source note | uspto-grants-1986_10 |