Methyl iodide → HCID 86741081, compound

Participants

Reaction Steps

A mixture of 0.2 g of 5-(3-fluoro-4-phenyl-α-methylbenzyl)-3-(2-methylthioethyl)-1,2,4-oxadiazole and 2 ml of methyl iodide was stirred and refluxed for 10 hours. After the mixture was concentrated to dryness under reduced pressure, the residue was triturated with diethyl ether, collected by filtration and dried to give [5-(3-fluoro-4-phenyl-α-methylbenzyl)1,2,4-oxadiazol-3-ylethyl]dimethylsulfonium iodide as light yellow fine crystals, m.p. 196.5° C. (decomp.).

Provenance & Evidence