HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13579603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Metaperiodic acid | HCID 65185 | — |
| Reactant | HCID 57164991 | HCID 57164991 | — |
| Product | HCID 13579603 | HCID 13579603 | 59.5% |
Reaction Steps
At first, 205 mg of compound (III) is dissolved in 3 ml of water, and 202 mg of periodic acid is added thereto. The mixture is stirred at room temperature for 1 hour and 30 minutes, and then chromatographically purified (HP-20SS 20 ml, water : methanol=4:1) to obtain 101 mg of compound (I) (59.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618687 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-b9fcbf58be334bcc8fe75778eecbd793 |
| Source note | uspto-grants-1986_10 |