HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Bis(benzyloxy)benzaldehyde → HCID 13565957, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Bis(benzyloxy)benzaldehyde | HCID 79526 | — |
| Reactant | Magnesium | HCID 5462224 | — |
| Reactant | HCID 19823699 | HCID 19823699 | — |
| Product | HCID 13565957 | HCID 13565957 | 18.5% |
Reaction Steps
By following the procedure as in Reference Example 25 using a Grignard reagent prepared from 3 g of 3,4-dibenzyloxybenzaldehyde, 2.5 g of 2-methyl-(7-bromoheptyl)-1,3-dioxolane, and 0.3 g of magnesium, 0.8 g of 1-(3,4-dibenzyloxyphenyl)-1,9-decanedione was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618627 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-58e65a48d968486cabd3e8a0ba65a118 |
| Source note | uspto-grants-1986_10 |