HCID 13746018, compound → HCID 13746019, compound

Participants

Reaction Steps

A mixture of the compound of example 14 (1.83 g, 4.5 mmole), 2 g of Raney Nickel, and 250 mL of 2-methoxyethanol was hydrogenated at 3 atmospheres in a Parr shaker for 0.5 hour. The resulting mixture was filtered and evaporated to give 1.8 g (71%) as a brown oil; M+ 380.

Provenance & Evidence