Iodoethane → HCID 20230753, compound

HRID 2290932Notes

Reaction equation

[CH3:1][O:2][C:3]1[C:15]2[CH2:14][CH2:13][CH:12]3[CH:8]([C:9](=[O:17])[NH:10][C:11]3=[O:16])[C:7]=2[C:6]([CH3:18])=[CH:5][C:4]=1[O:19][CH3:20].[CH2:21](I)[CH3:22]>>[CH2:21]([N:10]1[C:9](=[O:17])[CH:8]2[CH:12]([CH2:13][CH2:14][C:15]3[C:3]([O:2][CH3:1])=[C:4]([O:19][CH3:20])[CH:5]=[C:6]([CH3:18])[C:7]=32)[C:11]1=[O:16])[CH3:22]

Participants

Reactant 2

HCID 6340Iodoethane

HCID 13746030HCID 13746030, compound

Product 1

HCID 20230753HCID 20230753, compound

Procedure

Using the procedure as described for Example 64, but starting with 3,3a,4,5-tetrahydro-6,7-dimethoxy-9-methyl-1H-benz[e]isoindole-1,3-(2H)-dione, and using ethyl iodide in place of methyl iodide afforded the desired compound.

Sources & evidence

ORD record: ord-8d1ff1cafd74401cb9773de31ec91df2
Source dataset: uspto-grants-1986_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04618683

Reaction notes

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