Iodoethane → HCID 13746050, compound

HRID 2290938Notes

Reaction equation

HRID 2290938 reaction equation
[Br:1][C:2]1[C:14]2[CH2:13][CH2:12][CH:11]3[CH:7]([C:8](=[O:16])[NH:9][C:10]3=[O:15])[C:6]=2[C:5]([O:17][CH3:18])=[CH:4][CH:3]=1.[CH2:19](I)[CH3:20]>>[Br:1][C:2]1[C:14]2[CH2:13][CH2:12][CH:11]3[CH:7]([C:8](=[O:16])[N:9]([CH2:19][CH3:20])[C:10]3=[O:15])[C:6]=2[C:5]([O:17][CH3:18])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 13746045HCID 13746045, compound

Product 1

HCID 13746050HCID 13746050, compound

Procedure

Using the procedure of example 64, but starting with 6-bromo-3a,4,5,9b-tetrahydro-9-methoxy-1H-benz[e]isoindole-1,3-(2H)-dione and ethyl iodide instead of methyl iodide afforded the desired compound; M+ 337; mp 170°-4°.

Sources & evidence

ORD record
ord-90fbb514cb21486a9b5032312cede79a
Source dataset
uspto-grants-1986_10
Patent number
US04618683

Reaction notes

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