反应详情

温度

80 °C

Into a two liter reaction vessel equipped with stirrer, thermometer, heating mantel and reflux condenser is placed 1000 grams (7.35 moles) of 2-pentene-1,4-diol and 15 grams of boron trifluoride etherate. The reaction mass is then heated to 80° C. Over a period of two hours while maintaining the reaction mass at 80° C., 500 grams (3.7 moles) of camphene is added. The reaction is continued to be stirred at 80° C. for a period of 12.5 hours after the feeding of the camphene.

1. customInto a two liter reaction vessel
2. customequipped with stirrer
3. temperaturethermometer, heating mantel
4. temperaturereflux condenser
5. temperatureOver a period of two hours while maintaining the reaction mass at 80° C.