Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Camphene | HCID 6616 | — |
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | Pent-2-ene-1,4-diol | HCID 54161810 | — |
| Product | 4-(2-Bornyloxy)-2-buten-1-OL | HCID 54414726 | — |
Reaction Steps
Into a two liter reaction vessel equipped with stirrer, thermometer, heating mantel and reflux condenser is placed 1000 grams (7.35 moles) of 2-pentene-1,4-diol and 15 grams of boron trifluoride etherate. The reaction mass is then heated to 80° C. Over a period of two hours while maintaining the reaction mass at 80° C., 500 grams (3.7 moles) of camphene is added. The reaction is continued to be stirred at 80° C. for a period of 12.5 hours after the feeding of the camphene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04619780 |
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| Source dataset | uspto-grants-1986_10 |
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| ORD ID | ord-ca3c225fcf5a41f3b7491f8e22997145 |
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| Source note | uspto-grants-1986_10 |
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