Hydrochloric Acid → HCID 21279514, compound

HRID 2291213Notes

Reaction equation

HRID 2291213 reaction equation
[CH2:1]([S:8][C:9]1[N:13]=[C:12]([S:14][CH2:15][CH:16]([O:19]C)OC)[NH:11][N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl>CCOCC>[CH2:1]([S:8][C:9]1[N:13]=[C:12]2[S:14][CH2:15][CH:16]([OH:19])[N:11]2[N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21279510HCID 21279510, compound

Product 1

HCID 21279514HCID 21279514, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The product of stage (a) was heated under reflux with dilute hydrochloric acid (15 ml conc. plus 100 ml water) for 3 hours. The mixture was then cooled and stirred with ether. The precipitated solid was filtered off to give 5.4 g of desired product, mp 136°-138° C.

Workup

  1. temperatureThe mixture was then cooled
  2. filtrationThe precipitated solid was filtered off

Sources & evidence

ORD record
ord-22450bb098834f4091b5a9ae20c4e86d
Source dataset
uspto-grants-1989_01
Patent number
US04795483

Reaction notes

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