HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 131715805, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 1,1,1-Trifluoro-2-isothiocyanatoethane | HCID 13883777 | — |
| Reactant | HCID 21279726 | HCID 21279726 | — |
| Product | HCID 131715805 | HCID 131715805 | — |
Reaction Steps
A solution of 4-(2-aminopyrid-6-ylthio)butyronitrile (36 g.) and 2,2,2-trifluoroethylisothiocyanate (22 ml.) in acetonitrile (100 ml.) was left at room temperature for 18 hours. The crystalline precipitate was collected and washed with cold EtOH to give 4-[2-(3-[2,2,2-trifluoroethyl]thioureidopyrid-6-ylthio]butyronitrile, m.p. 131°-133°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04795755 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-4f35f14d5809445e8cce7da8126d050a |
| Source note | uspto-grants-1989_01 |