HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14648884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-(3,4-Dimethoxyphenyl)cyclohexanecarbonitrile | HCID 4639353 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 14648882 | HCID 14648882 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14648884 | HCID 14648884 | — |
Reaction Steps
A solution of 4-(3,4-dimethoxyphenyl)-4-cyanocyclohexane (5 mmol), N-(1-methylethyl)-4-(3,4-dimethoxyphenyl) butylamine hydrochloride (5 mmol), triethylamine (6 mmol) and sodium cyanoborohydride (6 mmol) in 25 ml ethanol was stirred at 25° C. for 72 hours and worked up and recrystallized. ##STR8##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04795757 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-a2d0f402b9104a2da40b7fa9e91e658f |
| Source note | uspto-grants-1989_01 |