HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 14648900, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Tetralone | HCID 68266 | — |
| Reactant | Cyclohexanecarbonitrile, 1-(3,4-dimethoxyphenyl)-4-oxo- | HCID 749913 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 22583-91-1 | HCID 12843075 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14648900 | HCID 14648900 | — |
Reaction Steps
A solution of 4-(3,4-dimethoxyphenyl)-4-cyanocyclohexanone (3 mmol), triethylamine (3 mmol), 2-ethylamino-1,2,3,4-tetrahydronaphthalene hydrochloride prepared by reductive amination of 3,4-dihydro-2-(1H)-naphthalenone with ethylamine and sodium cyanoborhydride, (3 mmol) in ethanol was stirred 72 hours and worked up as in Example 17. ##STR22##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04795757 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-aea211041d36403498231e5281873087 |
| Source note | uspto-grants-1989_01 |