HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 4-(Bromomethyl)-2,2-dimethyl-1,3-dioxolane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 3-Bromo-1,2-propanediol | HCID 20827 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Product | 4-(Bromomethyl)-2,2-dimethyl-1,3-dioxolane | HCID 169759 | — |
Reaction Steps
An acetone solution of bromomethyl ethylene glycol is refluxed for 24 hours in the presence of anhydrous magnesium sulfate. The cooled reaction mixture is filtered and the solvent is removed to provide a residual crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04796976 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-1b8c97ef73d242aa8fe5027e9c600a21 |
| Source note | uspto-grants-1989_01 |