HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 14013804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 3-Ethyl 5-methyl 4-chloro-6-(chlorodifluoromethyl)-2-(trifluoromethyl)-3,5-pyridinedicarboxylate | HCID 14013759 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14013804 | HCID 14013804 | 82.3% |
Reaction Steps
This compound was prepared as described in Example 37: 5.0 g (0.013 mol) of product of Example 28, 2.6 ml (0.025 mol) of diethylamine in 25 ml of DMF were reacted at room temperature for 16 hours affording a yellow semi-solid oil which was kugelrohr distilled at 80 Pa, pot temperature 102°-105° C. , to give 4.63 g (82.3%) of product as a yellow solid; mp 31.5°-33° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04797149 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-f23bf3002c734b7eb14baaf101a78d0b |
| Source note | uspto-grants-1989_01 |