Hydrogen Bromide → HCID 131715809, compound

HRID 2291534Notes

Reaction equation

HRID 2291534 reaction equation
[N+:1]([C:4]1[N:5]([CH2:9][CH:10]([OH:18])[CH2:11][N:12]2[CH2:17][CH:16]3[CH:14]([O:15]3)[CH2:13]2)[CH:6]=[CH:7][N:8]=1)([O-:3])=[O:2].[BrH:19]>C(O)C>[BrH:19].[N+:1]([C:4]1[N:5]([CH2:9][CH:10]([OH:18])[CH2:11][N:12]2[CH2:13][CH:14]3[CH:16]([O:15]3)[CH2:17]2)[CH:6]=[CH:7][N:8]=1)([O-:3])=[O:2]

Participants

4

Reactant 2

HCID 260Hydrogen BromideHCID 14373363HCID 14373363, compound

Product 1

HCID 131715809HCID 131715809, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

To a warm solution of 0.2 g of α-[(2-Nitro-1H-imidazol-1-yl)methyl)-6-oxa-3-azabicyclo[3.1.0]-hexane-3-ethanol in 3 ml of ethanol was added excess hydrogen bromide in ethanol. The solution was cooled and the resulting crystals collected to provide the title compound as the hydrobromide salt, mp 152-153 (dec).

Workup

  1. temperatureThe solution was cooled
  2. customthe resulting crystals collected

Sources & evidence

ORD record
ord-5515f84f67614f5c978f631bd6a671e9
Source dataset
uspto-grants-1989_01
Patent number
US04797397

Reaction notes

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