4-Nitrophenethyl bromide → HCID 21278911、化合物

関与物質

反応手順

The title compound, m.p. 102°-4°, was prepared similarly to the procedure of Example 1(A) from 1-(2-chloro-4-nitrophenyl)piperazine (1.2 g), 4-nitrophenethyl bromide (1.15 g) and sodium bicarbonate (0.85 g). The yield of the title compound was 0.37 g (from ethyl acetate), m.p. 100°-102°. A second batch had an m.p. of 102°-4° (from ethyl acetate/methanol)

情報源と証拠