HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → 1-(2-Chloro-4-methanesulphonamidophenyl)-4-(4-methanesulphonamidophenethyl)piperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 4-[4-[2-(4-Aminophenyl)ethyl]-1-piperazinyl]-3-chlorobenzenamine | HCID 21278905 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 1-(2-Chloro-4-methanesulphonamidophenyl)-4-(4-methanesulphonamidophenethyl)piperazine | HCID 21278915 | 64.2% |
Reaction Steps
The title compound (0.52 g), was prepared similarly to the procedure of Example 1(C) from methanesulphonyl chloride (0.44 g), 1-(4-amino-2-chlorophenyl)-4-(4-aminophenethyl)piperazine (0.55 g), and pyridine (10 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04797401 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-63693c7948bb4a5c9127d8fc249a2861 |
| Source note | uspto-grants-1989_01 |