HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21278917, compound → HCID 21278923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21278917 | HCID 21278917 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 21278923 | HCID 21278923 | — |
Reaction Steps
1-(3-Fluoro-4-nitrophenyl)-4-(4-nitrophenethyl)piperazine (0.19 g) and 10% palladium on carbon (150 mg) were hydrogenated at 4 atmospheres and 60° until completion of hydrogen uptake. The catalyst was then filtered off, the solvent evaporated, and the residual product (0.06 g) used directly in the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04797401 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-32797d31e6e5405bbf5bd1e7790d982f |
| Source note | uspto-grants-1989_01 |