HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminopyridine → N,N-diphenyl-N'-(4-pyridinyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminopyridine | HCID 1727 | — |
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | N,N-Diphenylcarbamic chloride | HCID 65741 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N,N-diphenyl-N'-(4-pyridinyl)urea | HCID 21279137 | — |
Reaction Steps
Employing the general method of Example 1, 27.5 g (0.12 mol) of diphenylcarbamic chloride and 20 g (0.12 mol) of 4-aminopyridine were heated under reflux for two hours in 150 ml of chloroform containing 12.0 g (0.12 mol) of triethylamine to produce the title compound as a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04797419 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-de9a25dc27964b549edf0a05670e008e |
| Source note | uspto-grants-1989_01 |